List of works - Roccaldo Sardella

(S)-(-)-alpha,alpha-Di(2-naphthyl)-2-pyrrolidinemethanol, a useful tool to study the recognition mechanism in chiral ligand-exchange chromatography.

scientific article published in January 2007

Achiral-chiral two-dimensional chromatography of free amino acids in milk: A promising tool for detecting different levels of mastitis in cows.

scientific article published on 3 January 2015

Assessment of safety and efficiency of nitrogen organic fertilizers from animal-based protein hydrolysates--a laboratory multidisciplinary approach.

scientific article published on 12 July 2013

Asymmetric synthesis of the four diastereoisomers of a novel non-steroidal farnesoid X receptor (FXR) agonist: role of the chirality on the biological activity

scientific article

Binding modes identification through molecular dynamic simulations: A case study with carnosine enantiomers and the Teicoplanin A2-2-based chiral stationary phase

scientific article published on 29 February 2020

Chiral ligand-exchange separation and resolution of extremely rigid glutamate analogs: 1-aminospiro[2.2]pentyl-1,4-dicarboxylic acids

scientific article published on 22 May 2010

Chiral mobile phase in ligand-exchange chromatography of amino acids: Exploring the copper(II) salt anion effect with a computational approach ⬇️

scientific article published on August 16, 2012

Chiral separation of helical chromenes with chloromethyl phenylcarbamate polysaccharide-based stationary phases.

scientific article published on 12 December 2017

Chromatographic separation and biological evaluation of benzimidazole derivative enantiomers as inhibitors of leukotriene biosynthesis

scientific article published on 07 November 2013

Chromatographic separation of free dafachronic acid epimers with a novel triazole click quinidine-based chiral stationary phase

scientific article published on 06 March 2014

Combined monodimensional chromatographic approaches to monitor the presence of d-amino acids in cheese

Computational studies for the elucidation of the enantiomer elution order of amino acids in chiral ligand-exchange chromatography

scientific article published on 08 October 2010

Continuous flow synthesis and scale-up of glycine- and taurine-conjugated bile salts

scientific article published on 19 April 2012

Correlation between CMC and chromatographic index: simple and effective evaluation of the hydrophobic/hydrophilic balance of bile acids

scientific article published on 16 June 2007

Cysteine-based chiral selectors for the ligand-exchange separation of amino acids.

scientific article published in November 2008

Derived chromatographic indices as effective tools to study the self-aggregation process of bile acids

scientific article published on 06 November 2008

Descriptive structure-separation relationship studies in chiral ligand-exchange chromatography.

scientific article published in July 2008

Determination of bile salt critical micellization concentration on the road to drug discovery

scientific article published on 04 July 2013

Diastereo- and enantioseparation of a Nα-Boc amino acid with a zwitterionic quinine-based stationary phase: Focus on the stereorecognition mechanism

scientific article published on 09 June 2015

Direct HPLC separation of carnosine enantiomers with two chiral stationaryn phases based on penicillamine and teicoplanin derivatives.

scientific article published on 12 December 2017

Direct chromatographic enantioresolution of fully constrained β-amino acids: exploring the use of high-molecular weight chiral selectors.

scientific article published on 6 February 2014

Direct enantioseparation of underivatized aliphatic 3-hydroxyalkanoic acids with a quinine-based zwitterionic chiral stationary phase

scientific article published on 30 March 2014

Discovery of 6alpha-ethyl-23(S)-methylcholic acid (S-EMCA, INT-777) as a potent and selective agonist for the TGR5 receptor, a novel target for diabesity.

scientific article published in December 2009

Dynamic ligand-exchange chiral stationary phase from S-benzyl-(R)-cysteine

scientific article published on 01 August 2006

Electrostatic attraction-repulsion model with Cinchona alkaloid-based zwitterionic chiral stationary phases exemplified for zwitterionic analytes

scientific article published on 05 June 2019

Enantioresolution and stereochemical characterization of two chiral sulfoxides endowed with COX-2 inhibitory activity.

scientific article published on 5 July 2017

Enantioresolution, stereochemical characterization and biological activity of a chiral large-conductance calcium-activated potassium channel opener

Enantioselective HPLC of potentially CNS-active acidic amino acids with a Cinchona carbamate based chiral stationary phase.

scientific article published in March 2008

Enantioseparations by high-performance liquid chromatography based on chiral ligand-exchange

scientific article published on 01 January 2013

Evaluation of the enantiomeric selectivity in the chiral ligand-exchange chromatography of amino acids by a computational model

scientific article published on 01 April 2004

Exploring the enantiorecognition mechanism of Cinchona alkaloid-based zwitterionic chiral stationary phases and the basic trans-paroxetine enantiomers.

scientific article

GC-MS/MS detects potential pregabalin abuse in susceptible subjects' hair

scientific article

Glucuronidation of bile acids under flow conditions: design of experiments and Koenigs-Knorr reaction optimization

scientific article published on 23 October 2014

HPLC/ELSD analysis of amidated bile acids: an effective and rapid way to assist continuous flow chemistry processes

scientific article published on 10 August 2012

Hydrophobic Amino Acid Content in Onions as Potential Fingerprints of Geographical Origin: The Case of

scientific article published on 25 May 2018

Ketoprofen enantioseparation with a Cinchona alkaloid based stationary phase: enantiorecognition mechanism and release studies.

scientific article

Last ten years (2008-2018) of chiral ligand-exchange chromatography in HPLC: An updated review

scientific article published on 12 September 2018

Liquid chromatography separation of α- and γ-linolenic acid positional isomers with a stationary phase based on covalently immobilized cellulose tris(3,5-dichlorophenylcarbamate)

scientific article published on 15 August 2019

Mechanistic considerations of enantiorecognition on novel Cinchona alkaloid-based zwitterionic chiral stationary phases from the aspect of the separation of trans-paroxetine enantiomers as model compounds

scientific article published on 27 February 2016

N-Decyl-S-trityl-(R)-cysteine, a new chiral selector for "green" ligand-exchange chromatography applications

scientific article published on 5 February 2017

Novel orthogonal liquid chromatography methods to dose neurotransmitters involved in Parkinson's disease.

scientific article published on 23 May 2014

Novel stereoselective synthesis and chromatographic evaluation of E-guggulsterone

scientific article published on 03 December 2011

Onion ( L.) Skin: A Rich Resource of Biomolecules for the Sustainable Production of Colored Biofunctional Textiles

scientific article published on 11 February 2019

Preparative resolution of 1-aminoindan-1,5-dicarboxylic acid (AIDA) by chiral ligand-exchange chromatography.

scientific article published in May 2004

Pyrazole[3,4-e][1,4]thiazepin-7-one derivatives as a novel class of Farnesoid X Receptor (FXR) agonists

scientific article published on 20 April 2012

Quinine-Based Zwitterionic Chiral Stationary Phase as a Complementary Tool for Peptide Analysis: Mobile Phase Effects on Enantio- and Stereoselectivity of Underivatized Oligopeptides

scientific article published on 20 October 2015

S-trityl-(R)-cysteine, a multipurpose chiral selector for ligand-exchange liquid chromatography applications

scientific article published on January 2015

Side-chain modified bile acids: chromatographic separation of 23-methyl epimers

scientific article published on 01 June 2009

Simultaneous diastereo- and enantioseparation of farnesoid X receptor (FXR) agonists with a quinine carbamate-based chiral stationary phase

scientific article

Synthesis and chromatographic enantioresolution of anti-HIV quinolone derivatives

article

Synthesis and chromatographic resolution of conformationally constrained analogues of homotaurine

article by Maria Carmela Fulco et al published October 2009 in Tetrahedron

Synthesis and quantitative structure-property relationships of side chain-modified hyodeoxycholic acid derivatives.

scientific article published on 30 August 2013

The "racemic approach" in the evaluation of the enantiomeric NorA efflux pump inhibition activity of 2-phenylquinoline derivatives.

scientific article published on 4 July 2016

The Relationship between S. aureus and Branched-Chain Amino Acids Content in Composite Cow Milk

scientific article published on 16 November 2019

The effect of mobile phase composition in the enantioseparation of pharmaceutically relevant compounds with polysaccharide-based stationary phases.

scientific article

The effect of the copper(II) salt anion in the Chiral Ligand-Exchange Chromatography of amino acids.

scientific article

Use of a Zwitterionic Surfactant to Improve the Biofunctional Properties of Wool Dyed with an Onion (Allium cepa L.) Skin Extract

scientific article published on 28 October 2020

Use of an o-Benzyl-(S)-Serine Containing Eluent for the Efficient Ligand-Exchange Chromatography-Based Enantioseparation of Constrained Glutamate Receptor Ligands

article by Federica Ianni et al published December 2014 in Analytical Letters

List of works by Roccaldo Sardella

(S)-(-)-alpha,alpha-Di(2-naphthyl)-2-pyrrolidinemethanol, a useful tool to study the recognition mechanism in chiral ligand-exchange chromatography.

Achiral-chiral two-dimensional chromatography of free amino acids in milk: A promising tool for detecting different levels of mastitis in cows.

Assessment of safety and efficiency of nitrogen organic fertilizers from animal-based protein hydrolysates--a laboratory multidisciplinary approach.

Asymmetric synthesis of the four diastereoisomers of a novel non-steroidal farnesoid X receptor (FXR) agonist: role of the chirality on the biological activity

Binding modes identification through molecular dynamic simulations: A case study with carnosine enantiomers and the Teicoplanin A2-2-based chiral stationary phase

Chiral ligand-exchange separation and resolution of extremely rigid glutamate analogs: 1-aminospiro[2.2]pentyl-1,4-dicarboxylic acids

Chiral mobile phase in ligand-exchange chromatography of amino acids: Exploring the copper(II) salt anion effect with a computational approach ⬇️

Chiral separation of helical chromenes with chloromethyl phenylcarbamate polysaccharide-based stationary phases.

Chromatographic separation and biological evaluation of benzimidazole derivative enantiomers as inhibitors of leukotriene biosynthesis

Chromatographic separation of free dafachronic acid epimers with a novel triazole click quinidine-based chiral stationary phase

Combined monodimensional chromatographic approaches to monitor the presence of d-amino acids in cheese

Computational studies for the elucidation of the enantiomer elution order of amino acids in chiral ligand-exchange chromatography

Continuous flow synthesis and scale-up of glycine- and taurine-conjugated bile salts

Correlation between CMC and chromatographic index: simple and effective evaluation of the hydrophobic/hydrophilic balance of bile acids

Cysteine-based chiral selectors for the ligand-exchange separation of amino acids.

Derived chromatographic indices as effective tools to study the self-aggregation process of bile acids

Descriptive structure-separation relationship studies in chiral ligand-exchange chromatography.

Determination of bile salt critical micellization concentration on the road to drug discovery

Diastereo- and enantioseparation of a Nα-Boc amino acid with a zwitterionic quinine-based stationary phase: Focus on the stereorecognition mechanism

Direct HPLC separation of carnosine enantiomers with two chiral stationaryn phases based on penicillamine and teicoplanin derivatives.

Direct chromatographic enantioresolution of fully constrained β-amino acids: exploring the use of high-molecular weight chiral selectors.

Direct enantioseparation of underivatized aliphatic 3-hydroxyalkanoic acids with a quinine-based zwitterionic chiral stationary phase

Discovery of 6alpha-ethyl-23(S)-methylcholic acid (S-EMCA, INT-777) as a potent and selective agonist for the TGR5 receptor, a novel target for diabesity.

Dynamic ligand-exchange chiral stationary phase from S-benzyl-(R)-cysteine

Electrostatic attraction-repulsion model with Cinchona alkaloid-based zwitterionic chiral stationary phases exemplified for zwitterionic analytes

Enantioresolution and stereochemical characterization of two chiral sulfoxides endowed with COX-2 inhibitory activity.

Enantioresolution, stereochemical characterization and biological activity of a chiral large-conductance calcium-activated potassium channel opener

Enantioselective HPLC of potentially CNS-active acidic amino acids with a Cinchona carbamate based chiral stationary phase.

Enantioseparations by high-performance liquid chromatography based on chiral ligand-exchange

Evaluation of the enantiomeric selectivity in the chiral ligand-exchange chromatography of amino acids by a computational model

Exploring the enantiorecognition mechanism of Cinchona alkaloid-based zwitterionic chiral stationary phases and the basic trans-paroxetine enantiomers.

GC-MS/MS detects potential pregabalin abuse in susceptible subjects' hair

Glucuronidation of bile acids under flow conditions: design of experiments and Koenigs-Knorr reaction optimization

HPLC/ELSD analysis of amidated bile acids: an effective and rapid way to assist continuous flow chemistry processes

Hydrophobic Amino Acid Content in Onions as Potential Fingerprints of Geographical Origin: The Case of

Ketoprofen enantioseparation with a Cinchona alkaloid based stationary phase: enantiorecognition mechanism and release studies.

Last ten years (2008-2018) of chiral ligand-exchange chromatography in HPLC: An updated review

Liquid chromatography separation of α- and γ-linolenic acid positional isomers with a stationary phase based on covalently immobilized cellulose tris(3,5-dichlorophenylcarbamate)

Mechanistic considerations of enantiorecognition on novel Cinchona alkaloid-based zwitterionic chiral stationary phases from the aspect of the separation of trans-paroxetine enantiomers as model compounds

N-Decyl-S-trityl-(R)-cysteine, a new chiral selector for "green" ligand-exchange chromatography applications

Novel orthogonal liquid chromatography methods to dose neurotransmitters involved in Parkinson's disease.

Novel stereoselective synthesis and chromatographic evaluation of E-guggulsterone

Onion ( L.) Skin: A Rich Resource of Biomolecules for the Sustainable Production of Colored Biofunctional Textiles

Preparative resolution of 1-aminoindan-1,5-dicarboxylic acid (AIDA) by chiral ligand-exchange chromatography.

Pyrazole[3,4-e][1,4]thiazepin-7-one derivatives as a novel class of Farnesoid X Receptor (FXR) agonists

Quinine-Based Zwitterionic Chiral Stationary Phase as a Complementary Tool for Peptide Analysis: Mobile Phase Effects on Enantio- and Stereoselectivity of Underivatized Oligopeptides

S-trityl-(R)-cysteine, a multipurpose chiral selector for ligand-exchange liquid chromatography applications

Side-chain modified bile acids: chromatographic separation of 23-methyl epimers

Simultaneous diastereo- and enantioseparation of farnesoid X receptor (FXR) agonists with a quinine carbamate-based chiral stationary phase

Synthesis and chromatographic enantioresolution of anti-HIV quinolone derivatives

Synthesis and chromatographic resolution of conformationally constrained analogues of homotaurine

Synthesis and quantitative structure-property relationships of side chain-modified hyodeoxycholic acid derivatives.

The "racemic approach" in the evaluation of the enantiomeric NorA efflux pump inhibition activity of 2-phenylquinoline derivatives.

The Relationship between S. aureus and Branched-Chain Amino Acids Content in Composite Cow Milk

The effect of mobile phase composition in the enantioseparation of pharmaceutically relevant compounds with polysaccharide-based stationary phases.

The effect of the copper(II) salt anion in the Chiral Ligand-Exchange Chromatography of amino acids.

Use of a Zwitterionic Surfactant to Improve the Biofunctional Properties of Wool Dyed with an Onion (Allium cepa L.) Skin Extract

Use of an o-Benzyl-(S)-Serine Containing Eluent for the Efficient Ligand-Exchange Chromatography-Based Enantioseparation of Constrained Glutamate Receptor Ligands