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List of works by Anne Lesage

13C-detected through-bond correlation experiments for protein resonance assignment by ultra-fast MAS solid-state NMR.

scientific article published on 15 April 2013

A Slowly Relaxing Rigid Biradical for Efficient Dynamic Nuclear Polarization Surface-Enhanced NMR Spectroscopy: Expeditious Characterization of Functional Group Manipulation in Hybrid Materials

article by Alexandre Zagdoun et al published 17 January 2012 in Journal of the American Chemical Society

A general strategy for obtaining 19F-19F and 13C-19F residual dipolar couplings in perfluorocarbons from the NMR spectroscopy of liquid crystalline samples

scientific article published in June 2010

A highly ordered mesostructured material containing regularly distributed phenols: preparation and characterization at a molecular level through ultra-fast magic angle spinning proton NMR spectroscopy

A well-defined Pd hybrid material for the Z-selective semihydrogenation of alkynes characterized at the molecular level by DNP SENS.

scientific article published on 19 August 2013

A well-defined silica-supported tungsten oxo alkylidene is a highly active alkene metathesis catalyst

scientific article published on 13 December 2013

Amplifying dynamic nuclear polarization of frozen solutions by incorporating dielectric particles

scientific article published on 23 October 2014

Assigning powders to crystal structures by high-resolution (1)H-(1)H double quantum and (1)H-(13)C J-INEPT solid-state NMR spectroscopy and first principles computation. A case study of penicillin G.

scientific article published on 20 June 2006

Atomic Description of the Interface between Silica and Alumina in Aluminosilicates through Dynamic Nuclear Polarization Surface-Enhanced NMR Spectroscopy and First-Principles Calculations

scientific article published on 5 August 2015

Atomic-level organization of vicinal acid-base pairs through the chemisorption of aniline and derivatives onto mesoporous SBA15

Atomistic Description of Reaction Intermediates for Supported Metathesis Catalysts Enabled by DNP SENS

Atomistic Description of Reaction Intermediates for Supported Metathesis Catalysts Enabled by DNP SENS.

scientific article published on 8 March 2016

BDPA-Nitroxide Biradicals Tailored for Efficient Dynamic Nuclear Polarization Enhanced Solid-State NMR at Magnetic Fields up to 21.1 T

scientific article published on 05 October 2018

Backbone assignment of fully protonated solid proteins by 1H detection and ultrafast magic-angle-spinning NMR spectroscopy

scientific article

Band-selective 1H− 13C cross-polarization in fast magic angle spinning solid-state NMR spectroscopy

scientific article

Better characterization of surface organometallic catalysts through resolution enhancement in proton solid state NMR spectra

article by Frédéric Blanc et al published 13 November 2006 in Inorganic Chemistry

Carbon-13 Spectral Editing in Solid-State NMR Using Heteronuclear Scalar Couplings

scientific article published in 1998

Carbon-13 lineshapes in solid-state NMR of labeled compounds. Effects of coherent CSA-dipolar cross-correlation

scientific article published in May 2003

Characterization of different water pools in solid-state NMR protein samples

scientific article

Characterizing slight structural disorder in solids by combined solid-state NMR and first principles calculations

scientific article published in February 2009

Combination of DQ and ZQ coherences for sensitive through-bond NMR correlation experiments in biosolids under ultra-fast MAS

article by Amy L. Webber et al published 23 April 2012 in ChemPhysChem

Complete (1)H resonance assignment of beta-maltose from (1)H-(1)H DQ-SQ CRAMPS and (1)H (DQ-DUMBO)-(13)C SQ refocused INEPT 2D solid-state NMR spectra and first principles GIPAW calculations

scientific article published on 18 May 2010

Complicated acute myocardial infarction requiring mechanical ventilation in the intensive care unit: prognostic factors of clinical outcome in a series of 157 patients

scientific article published in January 2004

DNP NMR of Biomolecular Assemblies

Dendritic polarizing agents for DNP SENS

scientific article published on 22 August 2016

Detailed structural investigation of the grafting of [Ta(=CHtBu)(CH2tBu)3] and [Cp*TaMe4] on silica partially dehydroxylated at 700 degrees C and the activity of the grafted complexes toward alkane metathesis

scientific article published in October 2004

Direct observation of reaction intermediates for a well defined heterogeneous alkene metathesis catalyst

scientific article

Donor-acceptor stacking arrangements in bulk and thin-film high-mobility conjugated polymers characterized using molecular modelling and MAS and surface-enhanced solid-state NMR spectroscopy

scientific article published on 14 February 2017

Dynamic Nuclear Polarization Efficiency Increased by Very Fast Magic Angle Spinning

scientific article published on 10 July 2017

Dynamic Nuclear Polarization Enhanced MAS NMR Spectroscopy for Structural Analysis of HIV-1 Protein Assemblies

scientific article published on 28 December 2015

Dynamic Nuclear Polarization Enhanced Solid-State NMR Spectroscopy of Functionalized Metal-Organic Frameworks

article

Dynamic Nuclear Polarization Magic-Angle Spinning Nuclear Magnetic Resonance Combined with Molecular Dynamics Simulations Permits Detection of Order and Disorder in Viral Assemblies

scientific article published on 11 June 2019

Dynamic Nuclear Polarization-Enhanced Biomolecular NMR Spectroscopy at High Magnetic Field with Fast Magic-Angle Spinning

scientific article published on 22 March 2018

Dynamic nuclear polarization at 40 kHz magic angle spinning

scientific article published on April 2016

Dynamic nuclear polarization surface enhanced NMR spectroscopy

scientific article published on 21 March 2013

Dynamics of silica-supported catalysts determined by combining solid-state NMR spectroscopy and DFT calculations

scientific article published on 11 April 2008

Enhanced sensitivity in high-resolution 1 H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS

Expanding the horizons for structural analysis of fully protonated protein assemblies by NMR spectroscopy at MAS frequencies above 100 kHz

scientific article published on 3 July 2017

Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling

scientific article

Fast Resonance Assignment and Fold Determination of Human Superoxide Dismutase by High-Resolution Proton-Detected Solid-State MAS NMR Spectroscopy

scholarly article by Michael J. Knight et al published 13 October 2011 in Angewandte Chemie International Edition

Frozen Acrylamide Gels as Dynamic Nuclear Polarization Matrices

scientific article

Frozen Acrylamide Gels as Dynamic Nuclear Polarization Matrices

High resolution solid state NMR spectroscopy in surface organometallic chemistry: access to molecular understanding of active sites of well-defined heterogeneous catalysts

scientific article

High-resolution NMR correlation spectra of disordered solids

scientific article published in April 2003

High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR

article by Ivano Bertini et al published 2011 in Chemical Science

Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation

Homonuclear dipolar decoupling with very large scaling factors for high-resolution ultrafast magic angle spinning 1H solid-state NMR spectroscopy

article published in 2010

Hybrid polarizing solids for pure hyperpolarized liquids through dissolution dynamic nuclear polarization

scientific article

Hydrophobic radicals embedded in neutral surfactants for dynamic nuclear polarization of aqueous environments at 9.4 Tesla

article

Improved dynamic nuclear polarization surface-enhanced NMR spectroscopy through controlled incorporation of deuterated functional groups

scientific article published on 4 January 2013

Influences of Dilute Organic Adsorbates on the Hydration of Low-Surface-Area Silicates

scientific article

Insights into the structure and dynamics of measles virus nucleocapsids by 1H-detected solid-state NMR.

scientific article

Internalization of human 5-HT4a and 5-HT4b receptors is splice variant dependent

scientific article published on June 2004

Investigation of dipolar-mediated water-protein interactions in microcrystalline Crh by solid-state NMR spectroscopy

scientific article

Iridium(I)/N-Heterocyclic Carbene Hybrid Materials: Surface Stabilization of Low-Valent Iridium Species for High Catalytic Hydrogenation Performance

scientific article published on 4 September 2015

Large molecular weight nitroxide biradicals providing efficient dynamic nuclear polarization at temperatures up to 200 K.

scientific article

Local Structures and Heterogeneity of Silica-Supported M(III) Sites Evidenced by EPR, IR, NMR, and Luminescence Spectroscopies.

scientific article

MK-801 alters RGS2 levels and adenylyl cyclase sensitivity in the rat striatum

scientific article published in February 2005

Measuring Nano- to Microstructures from Relayed Dynamic Nuclear Polarization NMR

Metal-Metal Synergy in Well-Defined Surface Tantalum-Iridium Heterobimetallic Catalysts for H/D Exchange Reactions

scientific article published on 25 November 2019

Methane reacts with heteropolyacids chemisorbed on silica to produce acetic acid under soft conditions

scientific article

Molecular Level Characterization of the Structure and Interactions in Peptide-Functionalized Metal-Organic Frameworks.

scientific article published on 11 October 2016

Molecular understanding of the formation of surface zirconium hydrides upon thermal treatment under hydrogen of [([triple bond]SiO)Zr(CH2tBu)3] by using advanced solid-state NMR techniques

scientific article published in October 2004

Motional heterogeneity in single-site silica-supported species revealed by deuteron NMR.

scientific article published on 14 July 2009

NMR signatures of the active sites in Sn-β zeolite

scientific article published on 30 July 2014

Nature and structure of aluminum surface sites grafted on silica from a combination of high-field aluminum-27 solid-state NMR spectroscopy and first-principles calculations

scholarly article by Rachel Nathaniel Kerber et al published 18 April 2012 in Journal of the American Chemical Society

Neurotrophic and antileukemic daphnane diterpenoids from Synaptolepis kirkii

scientific article published in October 2002

Non-aqueous solvents for DNP surface enhanced NMR spectroscopy

scientific article

Observation of heteronuclear overhauser effects confirms the 15N-1H dipolar relaxation mechanism in a crystalline protein

scientific article

On the orientational dependence of resolution in 1H solid-state NMR, and its role in MAS, CRAMPS and delayed-acquisition experiments

One- and Two-Dimensional High-Resolution NMR from Flat Surfaces

scientific article published on 11 February 2019

Out-and-back 13C-13C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS.

scientific article published on 29 June 2013

Oxygen-17 dynamic nuclear polarisation enhanced solid-state NMR spectroscopy at 18.8 T.

scientific article

Perhydrocarbyl ReVII complexes: comparison of molecular and surface complexes

scientific article

Polarization transfer over the water-protein interface in solids

scientific article

Powder crystallography of pharmaceutical materials by combined crystal structure prediction and solid-state 1H NMR spectroscopy

scientific article published on 18 March 2013

Predictive morphology, stoichiometry and structure of surface species in supported Ru nanoparticles under H2 and CO atmospheres from combined experimental and DFT studies

scientific article

Preferential Siting of Aluminum Heteroatoms in the Zeolite Catalyst Al-SSZ-70

scientific article published on 26 March 2019

Quantitative analysis of backbone dynamics in a crystalline protein from nitrogen-15 spin-lattice relaxation

article

Rapid proton-detected NMR assignment for proteins with fast magic angle spinning

scientific article

Rational design of dinitroxide biradicals for efficient cross-effect dynamic nuclear polarization.

scientific article

Reactive surface organometallic complexes observed using dynamic nuclear polarization surface enhanced NMR spectroscopy

scientific article published on 15 August 2016

Recent advances in solid-state NMR spectroscopy of spin I=1/2 nuclei

scientific article published on 15 July 2009

Silica-surface reorganization during organotin grafting evidenced by ¹¹⁹Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges

scientific article published in September 2014

Solid-State Dynamic Nuclear Polarization at 9.4 and 18.8 T from 100 K to Room Temperature

scientific article published on 10 November 2015

Solid-phase polarization matrixes for dynamic nuclear polarization from homogeneously distributed radicals in mesostructured hybrid silica materials

scientific article

Solid-state NMR of a paramagnetic DIAD-FeII catalyst: sensitivity, resolution enhancement, and structure-based assignments

scientific article published in October 2006

Solvent suppression in DNP enhanced solid state NMR.

scientific article

Spin-state selection in solid-state NMR.

scientific article published in September 2003

Supported Ru olefin metathesis catalysts via a thiolate tether

scientific article published on 01 February 2019

Surface versus Molecular Siloxy Ligands in Well-Defined Olefin Metathesis Catalysts: [{(RO)3SiO}Mo(NAr)(CHtBu)(CH2tBu)]

scholarly article by Frédéric Blanc et al published 13 February 2006 in Angewandte Chemie International Edition

Synthesis of Deuterium-Labeled Cryptophane-A and Investigation of Xe@Cryptophane Complexation Dynamics by 1D-EXSY NMR Experiments

scientific article (publication date: April 2001)

Tailored Polarizing Hybrid Solids with Nitroxide Radicals Localized in Mesostructured Silica Walls

scholarly article by Daniel L. Silverio et al published 29 May 2017 in Helvetica Chimica Acta

The Structure of Molecular and Surface Platinum Sites Determined by DNP-SENS and Fast MAS 195Pt Solid-State NMR Spectroscopy

scientific article published on 22 October 2020

Three-Dimensional Structure Determination of Surface Sites

scientific article

Transverse dephasing optimised NMR spectroscopy in solids: natural-abundance 13C correlation spectra

scientific article published in June 2004

Transverse-Dephasing Optimized HomonuclearJ-Decoupling in Solid-State NMR Spectroscopy of Uniformly13C-Labeled Proteins

article published in 2009

Two-Photon Absorbing AIEgens: Influence of Stereoconfiguration on Their Crystallinity and Spectroscopic Properties and Applications in Bioimaging

scientific article published on 20 November 2020

Water-protein hydrogen exchange in the micro-crystalline protein crh as observed by solid state NMR spectroscopy

scientific article

Water-protein interactions in microcrystalline crh measured by 1H-13C solid-state NMR spectroscopy

scientific article published in November 2003

Weak and Transient Protein Interactions Determined by Solid-State NMR.

scientific article

Well-Defined Silica-Supported Mo-Alkylidene Catalyst Precursors Containing One OR Substituent: Methods of Preparation and Structure-Reactivity Relationship in Alkene Metathesis

Well-defined surface imido amido tantalum(v) species from ammonia and silica-supported tantalum hydrides

article

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